 |
|
Subject: bis-nitro alcohol chem. A solution of bis-nitro alcohol (6) (7.94 g, 11.6 mmol, 1 eq), tert-butyldimethylsilylchloride (4.54 g, 30.15 mmol, 2.6 eq) and imidazole (4.1 g, 60.3 mmol, 5.2 eq) in anhydrous DMF (100 mL) under an argon atmosphere was stirred at room temperature for 3 hours.бис-нитроспирт? (ссылок нет) |
| You need to be logged in to post in the forum |