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 Natuli

link 10.09.2010 21:03 
Subject: baseline begins to exhibit fluctuations and the MOPS the peaks begin to appear distorted. chromat.
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At 24%, the baseline begins to exhibit fluctuations and the MOPS peaks begin to appear distorted.

контекст: Chromatographic Robustness
Increase in % of acetonitrile will elute all peaks
earlier, sharpen the peak shapes between Х
and MOPS and decrease the separation between
Dimer I, II and У. At 24%, the
baseline begins to exhibit fluctuations and the MOPS
peaks begin to appear distorted. However, all system
suitability criteria are still met. Decrease in %
acetonitrile will decrease the separation between
Х and MOPS.
MOPS= 3-[N-morpholino]propanesulfonic acid, sodium salt

 OlgaAvdeeva

link 11.09.2010 12:43 
...нулевая линия становится неустойчивой, искажается форма пиков MOPS ...

 Natuli

link 11.09.2010 13:39 
Ольга спасибо за "неустойчивую нулевую линию"!

 

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